Making goldene has proven tough in the past because its atoms tend to clump together. So, even if you can create a 2D sheet of gold atoms they quickly roll up to create nanoparticles instead.
The researchers got around this by taking a ceramic called titanium silicon carbide, which features ultra-thin layers of silicon between layers of titanium carbide, and coating it with gold. They then heated it in a furnace, which caused the gold to diffuse into the material and replace the silicon layers in a process known as intercalation.
This created atomically thin layers of gold embedded in the ceramic. To get it out, they had to borrow a century-old technique developed by Japanese knife makers. They used a chemical formulation known as Murakami’s reagent, which etches away carbon residue, to slowly reveal the gold sheets.